Pry mounted fully transparent ultra-high temperature and high pressure reaction system

Pry mounted fully transparent ultra-high temperature and high pressure reaction system

Main reactor:

material;High pressure quartz, purity99.5%,；Positive pressure resistance:10bar；Negative pressure resistance:20pa

Inner kettle wall thickness:10mm；Inner diameter:120mm；Height:100mmOuter kettle wall thickness:10mm；Inner diameter:160mm；Height:100mm；Total volume: not less than1000ml

High temperature design:300℃, operating temperature below290℃, readability accuracy:0.01℃

Stable accuracy1%Within (except for situations without heat release or continuous vacuum, continuous pressure), other situations need to be calibrated according to the material, and suitable environmental conditions can be controlled within ±0.5 ℃

Lower the head without dead volume

High temperature type temperature sensor

High temperature pressure sensor

Radial high-temperature medium heat transfer component, used for high temperature in the middle and lower parts, to avoid excessive heat transfer and excessive heat loss

Cauldron strength:DN10真空管道，上通-0.098--1MpaPressure sensor (high temperature type)

Up to GermanyLanguagePositive and negative pressure integrated pressure gauge (high temperature type)

High temperature sealingOOne circular ring；fixing screwM6SS/4-6；Upper sealing clamp ring6set

One set of intake pipeline valve (including automatic negative pressure safety interlock explosion-proof)BT4Channel switch

One set of exhaust pipeline valves (including automatic positive pressure safety interlock explosion-proof)BT4Channel switch

DN10A set of vacuum high-temperature regulating ball valves

Material (liquid) addition leakage head,100mlIncluding cover, high temperature and pressure resistant valve

Cauldron cover: High temperature sealingOOne circular ring；One sealed horizontal groove；Hexagonal fixed installation hole6Axial force adjustment sealing support frame6Material of the set:310S

Axial adjustment pressure0-10Mpa；The axial adjustment spacing shall not be less than3cm；Axial adjustment of expansion coefficient25%within

Elastic components12only；Top thread fastener12only；Self made adjusting nut6set；LCorner fixed threaded component6set

定制 AED(Ether, Tetrafluoroethylene, Perfluoroene Ether)Ternary copolymer high-temperature sealing ring

Customized development mold: inner diameter120*wide width10mm --1only

inner diameter160*wide width10mm --1only

fully automaticPSEPressure safety controller: pressure relief and reduction below0.1Mpa,Under the condition of effectively maintaining overpressure discharge,

The reaction system is not destroyed ；

Constant pressure relief, constant temperature relief, timed relief, and cumulative relief; Unmanned safety and voltage stabilization; Interlocking constant pressure control of front and rear exhaust

Pry mounted fully transparent ultra-high temperature and high pressure reaction system

Mixing device:

High resistance negative pressure magnetic coupling stirring device；Magnetic coupling connecting shaft316LOne time precision machining, non welding

mixing motor; 200W；IPProtection level,IP67

Adjustable stirring speed30-1200RPMAdapt to viscosity5ten thousandCPWithin;

Equipped with high-temperature reaction cooling protective jacket,Including import and export pipes

Standard configuration: Cone bottom frame hybrid propeller, detachable and replaceable

Mixing blade: material316L；Coupling coupling1set：material316L

Bottom: Material:316L；Molding: Cone Bottom；Processing technology:CNCOne time nature, no welding；Installation groove for kettle body*2No explosive connection；Liquid flow hole*2place；Bottom with high-temperature jacket；Discharge head

Replace the jacket with a single-sided closure, allowing high-temperature media to flow in and out in one direction, and install internal flow guides

The jacket is a welded component:The inlet and outlet high-temperature medium valves are high-temperature alloy regulating on-off valves2only

Temperature sensor bottom in type

Bottom tray fixing plate, horizontally fixed, solves micro deformation

Sensor fixing kit

Bottom trayLCorner fixing kit

定制 AED(Ether, Tetrafluoroethylene, Perfluoroene Ether)Ternary copolymer high-temperature sealing ring

Customized development mold: inner diameter120*wide width10mm --1only

inner diameter160*wide width10mm --1only

High temperature controller:

Design temperature:RT-320℃ (depending on the upper limit of the high-temperature medium) plus

Thermal power not less than5KW

Built in temperature sensor: outlet/回口-Material temperature monitoring

Internal oil constant temperature accuracy±0.5℃, the optimal environmental conditions can reach

±0.1Programming function for multi-stage constant temperature process at ℃

Fully automatic water cooling (water source required)

Software adjustment function:

PIDSelf tuning function, self correction compensation function, manual compensation function, safety warning function, constant temperature time control function, constant temperature time period control function,

High temperature metal insulated conveying pipeline:1.5rice*2/Color distinction: Blue/red

Ultra high temperature heat transfer oil:Eurotherm 315，10LRecommended operating temperature:-25～315℃

Device framework: mainly aluminum alloy type

Manual force reduction self-locking lifting platform

Fixed frame for kettle lid；Pot body tray；Lift module；Manual handle

Tubular condenser

together10Tube, single tube length500mm；pipe diameter3/8''；Hollow refrigerant；Condensation area;1100cm2

Built in temperature sensor：Pry mounted fully transparent ultra-high temperature and high pressure reaction system

Parallel condensing collector ：1Connect the collector to the main condenser；500mlBuilt in circular condenser collection tube for volume

With a long viewing window：Lower outlet valve

Equipped with a low-temperature jacket, connected in series with the condenser at low temperatures

Isostatic pressure connection pipeline at the outlet, including a set of high-temperature valves

2Number collector connection1Number Collector

Built in circular condensation collection tube

Plays a secondary buffering and collection role

Lower outlet valve：500mlvolume

3Number receiver connection1Number Collector；Built in circular condensation collection tube；Plays a three-level buffering collection role

Lower outlet valve；1000mlvolume；The parallel collector connection pipe isDN20

Condenser low temperature controller: acts on the kettle lid stirring-Condenser series cooling

Fully enclosed low-temperature controller：control temperature-40℃-RT；Operating temperature-15℃-RT；Fully automatic water cooling (water source required)

software control

One set of industrial control box (data acquisition and processing, transmission, reaction system control, power distribution), equipped with emergency switch；One set of computer and software workstation for operation, placed in the non explosion proof area operation room

Pry mounted fully transparent ultra-high temperature and high pressure reaction system

Control function:

Control the target temperature setting for temperature rise

Control the stirring and mixing speed

Condensation temperature setting

Control the switch of the vacuum pump/Start-stop

Security function:

When the vacuum degree reaches the set value, the vacuum suction will automatically stop

When the vacuum degree is higher than the set value, automatically start vacuum suction

When the positive pressure value reaches the safe value, it will automatically release pressure

When the positive pressure value is lower than the safe value, the pressure relief valve will automatically close

Recording function:

Record the negative pressure curve of the vacuum process and save it for long-term viewing

Record the heating process curve and save it for long-term viewing

Record the temperature change process of the condenser and store it for a long time for viewing

Record the negative pressure curve during the positive pressure process and save it for long-term viewing

Remote function:

Through remote control software, achieve operation control and power on/off of on-site equipment

(Need to be inwindowsRemote connection on computer, with network required)