High pressure reactor

High pressure reactorProduct Introduction:

CJFSeries Laboratory Magnetic Stirring Reactor Gas-Liquid, liquid-Liquid, liquid-Solid or gas-liquid-A stirring reaction device for chemical reactions of solid three-phase chemical materials can fully stir various chemical materials under high pressure, vacuum, and temperature to enhance mass and heat transfer processes.

High pressure reactorProduct Features:

The main feature of this device is the use of a static sealing structure, with a magnetic coupling connection between the stirring shaft and the motor drive. Due to its non-contact torque transmission, static sealing replaces dynamic sealing, which can solve the leakage problem of stirring and keep the entire medium and stirring components in a sealed state for operation. Therefore, it is more suitable for stirring reactions in various flammable, explosive, highly toxic, valuable media and other highly permeable chemical media. It is an ideal leak free reaction equipment for sulfurization, fluorination, hydrogenation, oxidation and other reactions in petroleum, chemical, organic synthesis, polymer material polymerization and other processes.

1The kettle body and lid are made of high-quality stainless steel processingHigh pressure reactorThe kettle body is connected to the flange through threads, and the kettle cover is a regular flat plate cover, which is fastened by main bolts and nuts evenly distributed in the circumferential direction;

2The main sealing of the pressure resistant kettle adoptsAThe double line seal of the model adopts a sealing form where the other sealing points are in line contact with the circular arc surface and the plane, and the circular arc surface is in line contact with the circular arc surface. By relying on the high precision and smoothness of the contact surface, a good sealing effect is achieved.

High pressure reactorProduct Structure:

The equipment mainly consists of three parts: tank body, heating, and mixing system:

1The main material and material contact parts of the stainless steel reaction kettle are both made of304or316LMade of high-quality stainless steel, in compliance withGMPStandard;

2The sealing adopts a hard seal, which can ensure the pressure inside the tank and prevent unnecessary pollution caused by material leakage inside the tank;

3The heating device adopts electric heating, which is convenient for hygiene;

4Anchor type or flip up type mixing blades are commonly used for mixing to ensure uniform mixing of materials.

Notes:

1The pressure resistant kettle is a sophisticated equipment that uses a conical contact sealing form through a sealing ring, and achieves sealing by tightening the main bolt to press them against each other. Special care must be taken for the sealing cone surface to avoid damage caused by various collisions. When installing the cover, first place the reaction kettle body, then carefully install the kettle cover in a fixed position on the kettle body. When tightening the main bolts, they must be tightened diagonally and symmetrically in multiple steps, with even force. The kettle cover is not allowed to tilt to one side to achieve good sealing effect, and the specified tightening torque should not be exceeded to prevent the sealing surface from being squeezed or accelerated wear;

2After each operation, the residue on the kettle body and lid should be removed. All sealing surfaces on the pressure resistant kettle should be cleaned regularly and kept dry. It is not allowed to use hard objects or soft objects with rough surfaces for cleaning;

3Strictly follow the "Regulations for Safe Use of High Temperature and Pressure Resistant Reactors" when operating the reactor, and do not operate it alone. Two or more people are required for the experiment;

4During the operation of the pressure vessel, turn on the ventilation fan to ensure good ventilation;

5When there is pressure inside the kettle, it is strictly prohibited to twist the nut or tap the pressure resistant kettle;

6At the connection between the positive and negative nuts (the intake pipe, exhaust pipe, and the branch pipe connecting the pressure gauge and the kettle cover), only the nut should be rotated, and the two sealing surfaces should not rotate relative to each other;

7Observe the reading of the pressure gauge at all times during operation, and it is strictly prohibited to use the kettle under conditions of overheating and overpressure;

8If there is any air leakage during the experiment, immediately stop heating and the experiment. It is strictly prohibited to twist the nut at high temperatures.

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